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HRID 1881624作成日:2026年10月25日

2-(3,4-Dichlorophenyl)-3-hydroxy-4-(methylcarbonyl)thiophene → Methyl 2-nitro-4-[(2-{1-[5-(3,4-dichlorophenyl)-4-hydroxy-3-thienyl]ethylidene}hydrazino)carbonyl]benzoate

https://huagongshe.com/reaction/1881624

反応式

関与物質

役割名称HCID仕込み量
反応物2-(3,4-Dichlorophenyl)-3-hydroxy-4-(methylcarbonyl)thiopheneHCID 44207288—
反応物4-Methoxycarbonyl-3-nitrobenzhydrazideHCID 66986356—
生成物Methyl 2-nitro-4-[(2-{1-[5-(3,4-dichlorophenyl)-4-hydroxy-3-thienyl]ethylidene}hydrazino)carbonyl]benzoateHCID 72360084—

反応手順

Using 2-(3,4-dichlorophenyl)-3-hydroxy-4-methylcarbonylthiophene (100 mg, 0.35 mmol) and methyl 2-nitro-4-hydrazinocarbonylbenzoate (93 mg, 0.39 mmol) as the starting materials, the desired product was obtained in the same manner as in Synthetic Example 65 as a yellow solid (147 mg, yield 83%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08318796B2
出典データセットuspto-grants-2012_11
ORD IDord-de6f79af1b57426b935a6e951322b54a
出典メモuspto-grants-2012_11