戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1881625作成日:2026年10月25日

2-(4-t-Butylphenyl)-3-hydroxy-4-methylcarbonylthiophene → Methyl 2-bromo-4-[(2-{1-[5-(4-t-butylphenyl)-4-hydroxy-3-thienyl]ethylidene}hydrazino)carbonyl]benzoate

https://huagongshe.com/reaction/1881625

反応式

関与物質

役割名称HCID仕込み量
反応物2-(4-t-Butylphenyl)-3-hydroxy-4-methylcarbonylthiopheneHCID 44207289—
反応物Methyl 2-bromo-4-hydrazinocarbonylbenzoateHCID 67050217—
生成物Methyl 2-bromo-4-[(2-{1-[5-(4-t-butylphenyl)-4-hydroxy-3-thienyl]ethylidene}hydrazino)carbonyl]benzoateHCID 72360105—

反応手順

Using 2-(4-t-butylphenyl)-3-hydroxy-4-methylcarbonylthiophene (55 mg, 0.20 mmol) and methyl 2-bromo-4-hydrazinocarbonylbenzoate (60 mg, 0.22 mmol) as the starting materials, the desired product was obtained in the same manner as in Synthetic Example 65 as a yellow solid (92 mg, yield 87%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08318796B2
出典データセットuspto-grants-2012_11
ORD IDord-5431ad90f806487995d561e70a30ab58
出典メモuspto-grants-2012_11