Acetic Acid → HCID 66917539, compound

Participants

Reaction Steps

A mixture comprising the product from Step 1 (1.34 g, 2.53 mmol) in 33% HBr in acetic acid (13.4 mL, 25.3 mmol) is stirred at room temperature overnight. The resulting suspension is diluted with DCM (10-20 mL) and filtered under vacuum. The recovered solid is dried under vacuum for 2 days to afford the title compound. [MH+ 331.16]

Provenance & Evidence