HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-3-methylbenzoic Acid → HCID 11680744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-3-methylbenzoic Acid | HCID 2759583 | — |
| Reactant | 1-Aminoindane, (S)- | HCID 7000084 | — |
| Product | HCID 11680744 | HCID 11680744 | 63% |
Reaction Steps
Prepared in a similar manner to example 4 using 4-methoxy-3-methylbenzoic acid and (S)-2,3-dihydro-1H-inden-1-amine. Yield 63%. 1HNMR (500 MHz, dMSO): δ 1.94-1.99 (m, 1H), 2.17 (s, 3H), 2.41-2.46 (m, 1H), 2.82-2.87 (m, 1H), 2.96-3.01 (m, 1H), 3.83 (s, 3H), 5.53-5.57 (dd, 1H), 6.98-6.99 (d, 1H), 7.16-7.23 (m, 3H), 7.26-7.27 (m, 1H), 7.75-7.80 (m, 2H), 8.54-8.55 (d, 1H). MS (M+H, 282).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08318947B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-1dce0b18baf647b9b2a6f59fe1e60e28 |
| Source note | uspto-grants-2012_11 |