HCID 58880180, compound → HCID 58880157, compound

Participants

Role	Name	HCID	Charge
Reactant	HCID 58880180	HCID 58880180	—
Reactant	3-(5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-yloxy)-N,N-dimethylpropan-1-amine	HCID 58880181	—
Product	HCID 58880157	HCID 58880157	—

Reaction Steps

The title compound was prepared from Compound 218 by using an analogous procedure to that outlined in the preparation of Compound 205. 1H NMR (400 MHz, Methanol-d4) δ 8.35 (s, 1H) 8.15 (m, 1H) 8.07 (m, 1H) 7.97 (m, 1H) 7.88 (t, J=8.0 Hz, 1H) 7.66 (s, 1H) 7.23 (d, J=8.36 Hz, 1H) 7.16 (d, J=8.36 Hz, 1H) 4.44 (t, J=5.8 Hz, 2H) 3.72 (t, J=8.0 Hz, 2H) 3.43 (q, J=7.32 Hz, 2H) 3.03 (s, 6H) 2.41 (m, 2H) 1.34 (t, J=7.32 Hz, 3H). [M+H] calc'd for C24H27ClN3O3S, 472; found, 472.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08318939B2
Source dataset	uspto-grants-2012_11
ORD ID	ord-45a26b7250d2441abc1420d1ccd68e24
Source note	uspto-grants-2012_11