HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 2-(1H-1,3-benzodiazol-2-yl)acetate → 2-Benzimidazol-2-yl-N-(4-cyano(3-pyridyl))acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 2-(1H-1,3-benzodiazol-2-yl)acetate | HCID 308071 | — |
| Reactant | Lithium Hexamethyldisilazide | HCID 2733832 | — |
| Reactant | 3-Aminopyridine-4-carbonitrile | HCID 10678219 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Benzimidazol-2-yl-N-(4-cyano(3-pyridyl))acetamide | HCID 12988782 | — |
Reaction Steps
LiHMDS (2.5 eq) was added to ethyl 2-benzimidazol-2-ylacetate (1.0 eq) in THF at −78° C. After 1 hour, 3-amino-4-cyanopyridine (0.8 eq) in THF was added. The resulting mixture was allowed to warm to room temperature overnight. The mixture was quenched with NH4Cl (aqueous saturated solution) and extracted with EtOAc. The organic layer washed with H2O and brine, dried over Na2SO4, filtered, and concentrated in vacuo to yield a brown solid. The crude material was purified by silica gel chromatography (5:1 EtOAc:hexane) to yield the desired product. LC/MS m/z 278.3 (MH+), Rt 1.88 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759417B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-094e9bec0c534d9799f241e0fae634c8 |
| Source note | uspto-grants-2004_07 |