HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6-Epoxycholest-7-en-3-ol → HCID 57311702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6-Epoxycholest-7-en-3-ol | HCID 125859 | — |
| Solvent | Potassium | HCID 5462222 | — |
| Product | HCID 57311702 | HCID 57311702 | 35.8% |
Reaction Steps
5,6β-Epoxy-5β-cholest-7-en-3β-ol [J. Org. Chem. 50 (1985), 1835] (150 mg) is dissolved in 2.5 ml of a potassium hydroxyde solution (5% in methanol). The reaction mixture is refluxed for one hour. Aqueous work-up, extraction with ethylacetate and column chromatography yields 5β-cholest-7-ene-3β,5β-diol (54 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759400B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-933004eb1a1442349f69882b0149051f |
| Source note | uspto-grants-2004_07 |