HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane,N-dimethylmethanamine (1:1) → HCID 21906216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane,N-dimethylmethanamine (1:1) | HCID 6327651 | — |
| Reactant | HCID 21906360 | HCID 21906360 | — |
| Product | HCID 21906216 | HCID 21906216 | 24.7% |
Reaction Steps
Using a similar procedure to that described in Example 47-D, N-(5-chloropyridin-2-yl)-2-[[1-(1-Boc-piperidin-4-yl)-ethyl]amino]-4-methoxycarbonylbenzamide (0.35 g, 0.68 mmol) and borane trimethylamine complex (0.15 g, 2.0 mmol) afforded 70 mg of the title compound. IS-MS, m/e 417 (m+1) Analysis for C21H25ClN4O3.2 HCl:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759414B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-de4ea8d1add744abb495cdccdb8a4088 |
| Source note | uspto-grants-2004_07 |