HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 178478551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Titanium Tetrachloride | HCID 24193 | — |
| Reactant | HCID 178516071 | HCID 178516071 | — |
| Product | HCID 178478551 | HCID 178478551 | — |
Reaction Steps
To a solution of 0.02 moles of 2-hydroxy pyridine and 0.02 moles of triethylamine in 50 mL of THF, a solution of 0.01 moles of titanium tetrachloride was added dropwise at 0° C. and stirred overnight at room temperature. After filtration, the THF solution was evaporated and the product was extracted from the residue. The product has the formula:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759493B1 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-2bba41fd572248b483f5c51c8831cf32 |
| Source note | uspto-grants-2004_07 |