HCID 86591894, compound → HCID 23510061, compound

Participants

Reaction Conditions

Reaction Steps

385 mg (1.217 mmol) of ethyl (2E)-3-(4-{[(allyloxy)carbonyl]amino}phenyl)-2-azidoprop-2-enoate was dissolved in 25 mL toluene (˜0.05M solution). The mixture was heated to 80° C. for 2 h, cooled, and concentrated. Purification by column chromatography, eluting with 25% ethyl acetate/hexane provided 134 mg of ethyl 6-{[(allyloxy)carbonyl]amino}-1H-indole-2-carboxylate as a yellow solid.

Provenance & Evidence