HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydroxy-11-cycloeicosenone → 2-Hydroxycyclooctadecanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydroxy-11-cycloeicosenone | HCID 67312852 | — |
| Reactant | 2-Hydroxy-9-cyclooctadecenone | HCID 69649678 | — |
| Product | 2-Hydroxycyclooctadecanone | HCID 9878887 | — |
Reaction Steps
2-Hydroxy-11-cycloeicosenone of Synthesis Example 7 was replaced by 2-hydroxy-9-cyclooctadecenone (1.0 g, 3.54 mmol), and a hydrogenation and subsequent treatment were performed under the same conditions as in Synthesis Example 7, to yield 1.0 g of 2-hydroxycyclooctadecanone (quantitative yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06759557B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-b77a471df5e74655ac77e43502bce19d |
| Source note | uspto-grants-2004_07 |