Hexylamine → HCID 9813085, compound

Participants

Reaction Steps

Using the general procedure, 4-bromobenzonitrile (182 mg, 1.0 mmol) was coupled with n-hexylamine (198 μL, 1.5 mmol). Purification of the crude product by column chromatography on silica gel using hexane/ethyl acetate (6:1) as eluent afforded the desired product as a light yellow solid (145 mg, 72% yield). Rf=0.6 (hexane/ethyl acetate=3:1).

Provenance & Evidence