Hexylamine → HCID 9964251, compound

Participants

Reaction Steps

Using the general procedure, 3-bromopyridine (96 μL, 1.0 mmol) was coupled with n-hexylamine (198 μL, 1.5 mmol) at 90° C. for 18 h. Purification of the crude product by column chromatography on silica gel using hexane/ethyl acetate (1:1) as eluent afforded the desired product as a colorless oil (146 mg, 82% yield). Rf=0.2 (hexane/ethyl acetate=2:1).

Provenance & Evidence