HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23508505, compound → HCID 23508424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23508505 | HCID 23508505 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 23508424 | HCID 23508424 | 92.3% |
Reaction Steps
A mixture composed of 350 mg of 4-[N-(4-benzyloxybenzyl)-N-methylsulfonylamino]phenyl methanesulfonate, 350 mg of 10% palladium-carbon, and 10 ml of dioxane was stirred for 2 days under an atmospheric pressure of hydrogen. The reaction mixture was filtered to remove any insoluble matter, and the solvent was distilled off from the filtrate. Thus, there was obtained 260 mg of 4-[N-(4-hydroxybenzyl)-N-methylsulfonylamino]phenyl methanesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762205B1 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-e709158e422a405eaf229008c5119fb2 |
| Source note | uspto-grants-2004_07 |