Methyl iodide → HCID 23508483, compound

HRID 1883675Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:19]=[CH:18][C:6]([C:7]([NH:9][C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([O:16][CH3:17])[CH:11]=2)=[O:8])=[CH:5][CH:4]=1.[CH3:20]I>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([N:9]([C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([O:16][CH3:17])[CH:11]=2)[CH3:20])=[O:8])=[CH:18][CH:19]=1

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 6870874-METHOXY-N-(3-METHOXYPHENYL)BENZAMIDE

Product 1

HCID 23508483HCID 23508483, compound

Procedure

The procedure of Preparation Example 14 was repeated, except that 4-methoxy-N-(3-methoxyphenyl)benzamide was used in place of 4-methoxy-N-(4-methoxyphenyl)benzamide, and 1.2 ml of methyl iodide was used in place of ethyl iodide. Thus, there was obtained 625 mg of 4-methoxy-N-(3-methoxyphenyl)-N-methylbenzamide.

Workup

customThe procedure of Preparation Example 14

Sources & evidence

ORD record: ord-ff887389f656422984122da6c98de7de
Source dataset: uspto-grants-2004_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06762205B1

Reaction notes

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