Iodoethane → HCID 23508428, compound

Participants

Reaction Steps

The procedure of Preparation Example 38 was repeated, except that 314 mg of 4-[N-(4-benzyloxybenzyl)amino]benzonitrile was used in place of 4-[N-(3-pyridyl)amino]benzonitrile, and 156 mg of ethyl iodide was used in place of 4-benzyloxybenzyl chloride. The resulting crude product was purified by TLC (using a 2:1 mixture of hexane and ethyl acetate as the developing solvent) to obtain 114 mg of 4-[N-(4-benzyloxybenzyl)-N-ethylamino]benzonitrile.

Provenance & Evidence