HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2Z)-2,3-bis(4-methoxyphenyl)prop-2-enenitrile → 92497-66-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2Z)-2,3-bis(4-methoxyphenyl)prop-2-enenitrile | HCID 5716814 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | 92497-66-0 | HCID 6303362 | 64.9% |
Reaction Steps
The procedure of Preparation Example 2 was repeated, except that 224 mg of (2Z)-2,3-bis(4-methoxyphenyl)prop-2-enenitrile was used in place of 4′-methoxy-2-biphenylacetonitrile, and 1,2-dichloroethane was used in place of methylene chloride. The resulting crude product was purified by TLC (using a 3:1 mixture of chloroform and acetone as the developing solvent) to obtain 130 mg of (2Z)-2,3-bis(4-hydroxyphenyl)-prop-2-enenitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762205B1 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-a6d7a8adb684455c8c7f7787a0305578 |
| Source note | uspto-grants-2004_07 |