Benzenemethanamine, 4-amino-N,N-dimethyl- → HCID 178468592, compound

HRID 1883777Notes

Reaction equation

HRID 1883777 reaction equation
C([N:4]1[C:12]2[C:7](=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH2:16][CH3:17])=[O:14])[CH:11]=2)[C:6](=[C:18](OCC)[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:5]1=[O:28])(=O)C.[CH3:29][N:30]([CH2:32][C:33]1[CH:39]=[CH:38][C:36]([NH2:37])=[CH:35][CH:34]=1)[CH3:31]>>[CH3:31][N:30]([CH2:32][C:33]1[CH:39]=[CH:38][C:36]([NH:37]/[C:18](=[C:6]2\[C:5](=[O:28])[NH:4][C:12]3[C:7]\2=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH2:16][CH3:17])=[O:14])[CH:11]=3)/[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:35][CH:34]=1)[CH3:29]

Participants

3

Reactant 2

HCID 308051Benzenemethanamine, 4-amino-N,N-dimethyl-HCID 685275611-Acetyl-3-(1-ethoxy-1-phenylmethylene)-6-ethoxycarbonyl-2-indolinone

Product 1

HCID 178468592HCID 178468592, compound

Procedure

Prepared from 1-acetyl-3-(1-ethoxy-1-phenylmethylene)-6-ethoxycarbonyl-2-indolinone and 4-(dimethylaminomethyl)-aniline Rf value: 0.7 (aluminium oxide, ethyl acetate/ethanol=20:1) C27H27N3O3

Sources & evidence

ORD record
ord-68b6f120da0c43b2ab3d7468d73886b1
Source dataset
uspto-grants-2004_07
Patent number
US06762180B1

Reaction notes

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