n-(3-Dimethylamino-propyl)-n-acetyl-p-phenylenediamine → HCID 178468599, compound

HRID 1883781Notes

Reaction equation

HRID 1883781 reaction equation
C([N:4]1[C:12]2[C:7](=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH2:16][CH3:17])=[O:14])[CH:11]=2)[C:6](=[C:18](OCC)[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[C:5]1=[O:28])(=O)C.[CH3:29][N:30]([CH3:45])[CH2:31][CH2:32][CH2:33][N:34]([C:38]1[CH:44]=[CH:43][C:41]([NH2:42])=[CH:40][CH:39]=1)[C:35](=[O:37])[CH3:36]>>[CH3:45][N:30]([CH3:29])[CH2:31][CH2:32][CH2:33][N:34]([C:38]1[CH:39]=[CH:40][C:41]([NH:42]/[C:18](=[C:6]2\[C:5](=[O:28])[NH:4][C:12]3[C:7]\2=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH2:16][CH3:17])=[O:14])[CH:11]=3)/[C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[CH:43][CH:44]=1)[C:35](=[O:37])[CH3:36]

Participants

3

Reactant 2

HCID 22668451n-(3-Dimethylamino-propyl)-n-acetyl-p-phenylenediamineHCID 685275611-Acetyl-3-(1-ethoxy-1-phenylmethylene)-6-ethoxycarbonyl-2-indolinone

Product 1

HCID 178468599HCID 178468599, compound

Procedure

Prepared from 1-acetyl-3-(1-ethoxy-1-phenylmethylene)-6-ethoxycarbonyl-2-indolinone and 4-(N-(3-dimethylamino-propyl)-N-acetyl-amino)-aniline Rf value: 0.2 (aluminium oxide, methylene chloride/ethanol=40:1) C31H34N4O4

Sources & evidence

ORD record
ord-eaf8e2ee82f546629bea3073c8c99dc5
Source dataset
uspto-grants-2004_07
Patent number
US06762180B1

Reaction notes

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