HuagongsheHuagongshe Chemistry Print Report · For research reference only
n-(3-Dimethylamino-propyl)-n-methylsulphonyl-p-phenylenediamine → methyl (3Z)-3-[[4-[3-(dimethylamino)propyl-methylsulfonylamino]anilino]-phenylmethylidene]-2-oxo-1H-indole-6-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | n-(3-Dimethylamino-propyl)-n-methylsulphonyl-p-phenylenediamine | HCID 23506963 | — |
| Reactant | 1-Acetyl-3-(1-ethoxy-1-phenylmethylene)-6-methoxycarbonyl-2-indolinone | HCID 66685972 | — |
| Product | methyl (3Z)-3-[[4-[3-(dimethylamino)propyl-methylsulfonylamino]anilino]-phenylmethylidene]-2-oxo-1H-indole-6-carboxylate | HCID 178497177 | — |
Reaction Steps
Prepared from 1-acetyl-3-(1-ethoxy-1-phenylmethylene)-6-methoxycarbonyl-2-indolinone and N-(3-dimethylamino-propyl)-N-methylsulphonyl-p-phenylenediamine Rf value: 0.5 (aluminium oxide, methylene chloride/methanol=30:1) C29H32N4O5S
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762180B1 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-2caca4173e4244198dbe195289999001 |
| Source note | uspto-grants-2004_07 |