N-cyclohexyl-p-phenylenedamine → HCID 178497172, compound

HRID 1883817Notes

Reaction equation

HRID 1883817 reaction equation
C([N:4]1[C:12]2[C:7](=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH3:16])=[O:14])[CH:11]=2)[C:6](=[C:17](OCC)[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:5]1=[O:27])(=O)C.[CH:28]1([NH:34][C:35]2[CH:40]=[CH:39][C:38]([NH2:41])=[CH:37][CH:36]=2)[CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]1>>[CH:28]1([NH:34][C:35]2[CH:36]=[CH:37][C:38]([NH:41]/[C:17](=[C:6]3\[C:5](=[O:27])[NH:4][C:12]4[C:7]\3=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH3:16])=[O:14])[CH:11]=4)/[C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=3)=[CH:39][CH:40]=2)[CH2:29][CH2:30][CH2:31][CH2:32][CH2:33]1

Participants

3

Reactant 2

HCID 2771376N-cyclohexyl-p-phenylenedamineHCID 666859721-Acetyl-3-(1-ethoxy-1-phenylmethylene)-6-methoxycarbonyl-2-indolinone

Product 1

HCID 178497172HCID 178497172, compound

Procedure

Prepared from 1-acetyl-3-(1-ethoxy-1-phenylmethylene)-6-methoxycarbonyl-2-indolinone and N-cyclohexyl-p-phenylenediamine Rf value: 0.8 (silica gel, methylene chloride/methanol=10:1) C29H28N2O3

Sources & evidence

ORD record
ord-45a7bf3dc5cb425486a1485b160510da
Source dataset
uspto-grants-2004_07
Patent number
US06762180B1

Reaction notes

Loading…