4-(1H-Imidazol-2-yl)aniline → HCID 178497127, compound
Reaction equation
C([N:4]1[C:12]2[C:7](=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH3:16])=[O:14])[CH:11]=2)[C:6](=[C:17](OCC)[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:5]1=[O:27])(=O)C.[NH:28]1[CH:32]=[CH:31][N:30]=[C:29]1[C:33]1[CH:39]=[CH:38][C:36]([NH2:37])=[CH:35][CH:34]=1>>[NH:28]1[CH:32]=[CH:31][N:30]=[C:29]1[C:33]1[CH:39]=[CH:38][C:36]([NH:37]/[C:17](=[C:6]2\[C:5](=[O:27])[NH:4][C:12]3[C:7]\2=[CH:8][CH:9]=[C:10]([C:13]([O:15][CH3:16])=[O:14])[CH:11]=3)/[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:35][CH:34]=1Participants
3
Procedure
Prepared from 1-acetyl-3-(1-ethoxy-1-phenylmethylene)-6-methoxycarbonyl-2-indolinone and 4-(imidazol-2-yl)-aniline Rf value: 0.5 (silica gel, methylene chloride/methanol=10:1) C26H20N4O3
Sources & evidence
- ORD record
- ord-8a04e3d4b5b8452aad37b33bd906c829
- Source dataset
- uspto-grants-2004_07
- Patent number
- US06762180B1
Reaction notes
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