HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluoronitrobenzene → 1-Fluoro-4-[(4-nitrophenoxy)methyl]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | 4-Fluorobenzylic alcohol | HCID 68022 | — |
| Reactant | 1-(3-Fluorobenzyloxy)-4-nitro-benzene | HCID 22137915 | — |
| Product | 1-Fluoro-4-[(4-nitrophenoxy)methyl]benzene | HCID 957511 | 86% |
Reaction Steps
The title compound is prepared in analogy to 1-(3-fluorobenzyloxy)-4-nitro-benzene, starting from 4-fluoro nitrobenzene and 4-fluoro benzyl alcohol. Yield: 86% of a slightly yellow solid. Mp.=124-126°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06762320B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-c02ce2bf6d1142ca9cf9af6eeac3257f |
| Source note | uspto-grants-2004_07 |