Ammonia → HCID 11723275, compound

HRID 1884145Notes

Reaction equation

HRID 1884145 reaction equation
C[O:2][C:3](=O)[CH2:4][C:5]([NH:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][C:16]2[CH:21]=[CH:20][CH:19]=[C:18]([F:22])[CH:17]=2)=[C:10]([CH3:23])[CH:9]=1)=[O:6].[NH3:25]>CO>[F:22][C:18]1[CH:17]=[C:16]([CH:21]=[CH:20][CH:19]=1)[CH2:15][O:14][C:11]1[CH:12]=[CH:13][C:8]([NH:7][C:5](=[O:6])[CH2:4][C:3]([NH2:25])=[O:2])=[CH:9][C:10]=1[CH3:23]

Participants

4

Reactant 2

HCID 222AmmoniaHCID 10065266HCID 10065266, compound

Product 1

HCID 11723275HCID 11723275, compoundYield 60%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Prepared in analogy to example 3 from N-[4-(3-fluoro-benzyloxy)-3-methyl-phenyl]-malonamic acid methyl ester and 7M ammonia in methanol. Yield=60%. Colorless solid. MS: m/e=317.0 (M++H).

Sources & evidence

ORD record
ord-2772b640a9b44abc819a89e1fa7e93c0
Source dataset
uspto-grants-2004_07
Patent number
US06762320B2

Reaction notes

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