2-Methyl-3-furanthiol → HCID 23508242, compound
Reaction equation
[CH3:1][C:2]1[O:3][CH:4]=[CH:5][C:6]=1[SH:7].[CH3:8][O:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[CH:21]=[CH:20][C:19]([S:22]([NH:25][CH:26]([CH2:31][CH:32]3[O:34][CH2:33]3)[C:27]([O:29]C)=[O:28])(=[O:24])=[O:23])=[CH:18][CH:17]=2)=[CH:12][CH:11]=1>>[CH3:8][O:9][C:10]1[CH:11]=[CH:12][C:13]([C:16]2[CH:17]=[CH:18][C:19]([S:22]([NH:25][CH:26]([CH2:31][CH:32]([OH:34])[CH2:33][S:7][C:6]3[CH:5]=[CH:4][O:3][C:2]=3[CH3:1])[C:27]([OH:29])=[O:28])(=[O:23])=[O:24])=[CH:20][CH:21]=2)=[CH:14][CH:15]=1Participants
3
Procedure
Example 43 is prepared from 2-methyl-3-furanthiol and 1d using the procedure described for compound 20.
Sources & evidence
- ORD record
- ord-bcf40a9b391f4127a4260ed0c673feee
- Source dataset
- uspto-grants-2004_07
- Patent number
- US06762198B2
Reaction notes
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