HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1884325Generated: October 25, 2026
Azobisisobutyronitrile → Acrylic acid methyl acrylate
https://huagongshe.com/reaction/1884325
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Propylene glycol methyl ether acetate | HCID 7946 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | Acrylic acid methyl acrylate | HCID 168350 | 54% |
Reaction Steps
9 g of acrylic acid, 1 g of methyl acrylate, 50 g of isobutyl methyl ketone, 50 g of propylene glycol methyl ether acetate and 3.0 g of AIBN were combined and heated to about 67° C. for 3 hours under an inert atmosphere (e.g., nitrogen gas). The precipitated polymer was washed with ethyl ether and vacuum dried to obtain pure poly(acrylic acid/methyl acrylate) resin (weight average molecular weight: 7200, yield: 54%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06764806B2 |
|---|
| Source dataset | uspto-grants-2004_07 |
|---|
| ORD ID | ord-c93311b8a222497fbf52377bc34c65e2 |
|---|
| Source note | uspto-grants-2004_07 |
|---|
