HuagongsheHuagongshe Chemistry Print Report · For research reference only
[-2,5,6-Trimethyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl]-propan-1-one oxime → 1-[2,5,6-Trimethyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl]-propylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [-2,5,6-Trimethyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl]-propan-1-one oxime | HCID 136388382 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-[2,5,6-Trimethyl-7-(2,4,6-trimethylphenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-yl]-propylamine | HCID 23505757 | — |
Reaction Steps
Hydrogenation of 1-[-2,5,6-Trimethyl-7-(2,4,6-trimethyl phenyl )-7H-pyrrolo[2,3-d]-pyrim-idin-4-yl]-propan-1-one oxime with 10% Pd/C in MeOH using the general procedure described in Example 29 resulted in the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06765008B1 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-d73a673fe37d48edb7b48ba7db7741d4 |
| Source note | uspto-grants-2004_07 |