HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1,3-Benzodioxol-5-amine, N-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1,3-Benzodioxol-5-amine | HCID 84310 | — |
| Product | 1,3-Benzodioxol-5-amine, N-methyl- | HCID 10606919 | 18% |
Reaction Steps
The title compound was prepared from 3,4-(methylenedioxy)aniline and iodomethane by the procedure described in example 2 in 18% yield. 1H NMR (CDCl3): 6.67 (d, J=8.3, 1H), 6.25 (d, J=2.2, 1H), 6.04 (dd, J=2.2, 8.3, 1H), 5.85 (s, 2H), 3.50 (br s, 1H), 2.79 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06765006B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-aa378083990849f0b32187b076a83abd |
| Source note | uspto-grants-2004_07 |