HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Diethylamino)-1-propanol → Diethyl-[3-(2-fluoro-4-nitro-phenoxy)-propyl]-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Diethylamino)-1-propanol | HCID 12159 | — |
| Reactant | 1,2-Difluoro-4-nitrobenzene | HCID 123053 | — |
| Product | Diethyl-[3-(2-fluoro-4-nitro-phenoxy)-propyl]-amine | HCID 21974931 | — |
Reaction Steps
In a manner similar to that described in Example 231 a, 3,4-difluoronitrobenzene (6.7 mL, 60.6 mmol, 1 equiv.) and 3-diethylamino-1-propanol (9 mL, 1 equiv.) are converted to the named compound as a brown oil (16.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06765012B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-b0ae79adeed04db3993d69a127a79789 |
| Source note | uspto-grants-2004_07 |