HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,1-dimethylindole-2-carboxamide → HCID 23505589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,1-dimethylindole-2-carboxamide | HCID 12303315 | — |
| Reactant | 1-(4-benzyloxybenzyl)-N-methylindole-2-carboxamide | HCID 23505575 | — |
| Product | HCID 23505589 | HCID 23505589 | 63.1% |
Reaction Steps
According to the procedure of Preparation 1 (b), except substituting 1-(4-benzyloxybenzyl)-N-methylindole-2-carboxamide (44.4 g, 120.1 mmole) for the N,1-dimethylindole-2-carboxamide, the title compound (27.0 g, 63%) was prepared as a white solid: MS (ES) m/e 358 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06765005B2 |
| Source dataset | uspto-grants-2004_07 |
| ORD ID | ord-4c08907027324cff9c03fca3103dba08 |
| Source note | uspto-grants-2004_07 |