4-Bromo-2,6-diiodophenol → (1,1':3',1''-Terphenyl)-2'-ol, 5'-phenyl-

Participants

Role	Name	HCID	Charge
Reactant	4-Bromo-2,6-diiodophenol	HCID 10287922	—
Reactant	N-(8-phenyl-octyl)-3,5-bis(m-trifluoromethylphenyl)4hydroxy-benzamide	HCID 22237600	—
Product	(1,1':3',1''-Terphenyl)-2'-ol, 5'-phenyl-	HCID 3623729	—

Reaction Steps

The title compound was prepared as a solid (0.055 g, 28%, product 2: tris-arylation) from 4-bromo-2,6-diiodophenol using the procedure to step 2 of Example 40; 1H NMR (CDCl3) δ 5.45 (s, 1H), 7.27-7.57 (m, 1 1H), 7.62 (d, J=8.3 Hz, 6H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06765021B2
Source dataset	uspto-grants-2004_07
ORD ID	ord-80d115ffed6e43979b9e59cdd3493b44
Source note	uspto-grants-2004_07