HRID1884830

反应详情

EQUATION

反应方程式

HRID 1884830 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

A mixture of the 3-(1-benzyl-1,2,5,6-tetrahydro-pyridin-3-yl)-1H-indole obtained in Example 28 and 10% palladium on carbon in a mixture of formic acid and methanol is stirred at room temperature for 3 days and filtered through celite. The celite is washed with methanol. The filtrates are combined and concentrated in vacuo to afford the title product, identified by HPLC and mass spectral analyses.

WORKUP

后处理

  1. filtrationfiltered through celite
  2. washThe celite is washed with methanol
  3. concentrationconcentrated in vacuo