Dihydrocoumarin → HCID 23505057, compound

Participants

Reaction Conditions

Reaction Steps

19.5 g of dihydrocoumarine was placed in a 250 ml round bottom flask with 20 ml of diallyl amine and 60 ml of toluene. The reaction mixture was stirred for 6 hrs at 50° C. The reaction mixture was then cooled, concentrated, and extracted with ethyl acetate and water. The organic phase was collected and concentrated to obtain dried solid. The obtained solid was recrystallized with ethyl acetate/n-hexane, filtered, washed with n-hexane, and vacuumed to dryness. 17.2 g of the product of formula (VIII) was obtained.

Provenance & Evidence