HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 19797774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Methyl 4-(bromomethyl)benzoate | HCID 256687 | — |
| Product | HCID 19797774 | HCID 19797774 | — |
Reaction Steps
2.61 g (11.4 mol) of methyl 4-(bromomethyl)benzoate (IV) synthesized in the 4th step and 3.0 g (11.45 mmol) of triphenylphosphine were dissolved in 100 ml of benzene, and the temperature was raised to the reflux temperature under stirring, at which temperature, the reaction was carried out for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05143644 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-50af0ba9ee1049f2be45ed7de927bd06 |
| Source note | uspto-grants-1992_09 |