HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 4-(acetyloxy)- → p-Acetoxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 4-(acetyloxy)- | HCID 16865 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | p-Acetoxybenzoyl chloride | HCID 2756254 | 104.3% |
Reaction Steps
10 g of p-acetyloxybenzoic acid was added to 45 ml of benzene, and 11.8 g of PCl5 was added little by little under stirring at room temperature. After 8.5 hours of heat-refluxing thereafter, the solvent was distilled off to obtain 11.5 g of p-acetyloxybenzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05143643 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-b70ede27eb5140309c2bbdf6c9ac60e9 |
| Source note | uspto-grants-1992_09 |