N,N-Dimethylaniline → HCID 19880043, compound

Participants

Reaction Steps

Separately, 9.0 g of 3-pentyloxybutanol and 6.82 g of N,N-dimethylaniline were added to 20 ml of ether, and under stirring at room temperature, 11.5 g p-acetyloxybenzoic acid chloride was added thereto dropwise. Then, the mixture was heat-refluxed for 3.5 hours. The crystal was dissolved by adding 50 ml of water and extracted with ether. The ether layer was washed successively with 10% H2SO4 aqueous solution and water and dried with anhydrous Na2SO4, followed by distilling-off of the solvent to obtain 17.5 g of 4-(3-pentyloxybutoxycarbonyl)phenyl acetate.

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