2-Thiophenecarbonyl chloride → HCID 19808468, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[N:13]2[CH2:18][CH2:17][N:16]([CH2:19][CH2:20][NH2:21])[CH2:15][CH2:14]2)=[CH:5][CH:4]=1.[S:22]1[CH:26]=[CH:25][CH:24]=[C:23]1[C:27]([Cl:29])=[O:28]>>[ClH:29].[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[N:13]2[CH2:18][CH2:17][N:16]([CH2:19][CH2:20][NH:21][C:27]([C:23]3[S:22][CH:26]=[CH:25][CH:24]=3)=[O:28])[CH2:15][CH2:14]2)=[CH:5][CH:4]=1Participants
3
Procedure
This compound was prepared according to the process described in Example 1, Stage E, from 1-(7-methoxy-1-naphthyl)-4-(2-aminoethyl)piperazine and 2-thiophenecarbonyl chloride.
Workup
- customThis compound was prepared
Sources & evidence
- ORD record
- ord-c7979546758b4b60b5ab8bc449fdb54f
- Source dataset
- uspto-grants-1992_09
- Patent number
- US05143916
Reaction notes
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