HCID 17943854, compound → HCID 10421501, compound

Participants

Reaction Steps

Cyclohexanone 4-nitro-3,5-dimethyl-1,2-phenylene ketal (10.0 g) and 10% palladium on charcoal (1.0 g) in ethanol (200 ml) was shaken in a hydrogen atmosphere (50 p.s.i.) at 45° C. for 3 hours. The mixture was filtered through celite and evaporated to leave cyclohexanone 4-amino-3,5-dimethyl-1,2-phenylene ketal (8.0 g, 90%) as a brown oil.

Provenance & Evidence