HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 19880151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methoxybenzyl bromide | HCID 165021 | — |
| Reactant | HCID 23435281 | HCID 23435281 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19880151 | HCID 19880151 | — |
Reaction Steps
Ethyl 5-chloro-3,4-dihydroxybenzoate is p-methoxybenzylated with p-methoxybenzyl bromide and potassium carbonate in dimethylformamide to give ethyl 5-chloro-3,4-bis(p-methoxybenzyloxy)benzoate. This is hydrolyzed with sodium hydroxide to give 5-chloro-3,4-di(p-methoxybenzyloxy)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05143910 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-f632d1f7ec5c4c5abc6e069827cb8e59 |
| Source note | uspto-grants-1992_09 |