HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1885819Generated: October 26, 2026
Thionyl Chloride → Chloromethyl chloroisopropyl benzene
https://huagongshe.com/reaction/1885819
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Chloro-3-isopropylbenzyl alcohol | HCID 14534574 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | Chloromethyl chloroisopropyl benzene | HCID 14555442 | 85.7% |
Reaction Steps
At room temperature, 29.8 g of thionyl chloride is carefully dripped into 35 g of 2-chloro-3-isopropylbenzyl alcohol in 80 ml of carbon tetrachloride. The mixture is stirred for 15 hours at 25° C. and then evaporated down. Distillation (bp 0.3 :76°-78° C.) gives 33 g of 2-chloro-3-isopropylbenzyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05147645 |
|---|
| Source dataset | uspto-grants-1992_09 |
|---|
| ORD ID | ord-fc3b6c140b8a4c1da8960675eeae99fb |
|---|
| Source note | uspto-grants-1992_09 |
|---|
