HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15107610, compound → HCID 14555435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15107610 | HCID 15107610 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladiumcarbon | HCID 14818447 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14555435 | HCID 14555435 | 49.8% |
Reaction Steps
103 g of 1-(3'-chloro-2'-methylphenyl)-cyclohexene is dissolved in 1,200 ml of ethanol; 5 g of Pd/charcoal is then added. Hydrogenation is then carried out for 8 hours at room temperature and a hydrogen pressure of 80 bar. The catalyst is filtered off and the remaining solution is evaporated down. Fractional distillation gives 51.8 g of 3-cyclohexyl-2-methylchlorobenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05147645 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-a27b8103273f430f8acaa719b0bb3f59 |
| Source note | uspto-grants-1992_09 |