HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminophenol → HCID 19878522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminophenol | HCID 5801 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13684698 | HCID 13684698 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19878522 | HCID 19878522 | 26.5% |
Reaction Steps
Using the general procedure of Example 1, 12.0 g (33 mmol) of 2,4,6-tri-tert-butylphenyl phosphorodichloridite, 3.6 g (33 mmol) of 2-aminophenol, 9.3 ml (66 mmol) of triethylamine and 75 ml of methylene chloride are reacted to give 3.5 g of the title compound as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05147909 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-ef545418cf564f5f87327cf6175fb6cf |
| Source note | uspto-grants-1992_09 |