3-Methylpentanoic acid → HCID 19876561, compound

HRID 1885955Notes

Reaction equation

[C:1]([C:4]1[CH:5]=[N:6][CH:7]=[CH:8][CH:9]=1)(=[O:3])[CH3:2].[CH3:10][CH:11]([CH2:16][CH3:17])[CH2:12][C:13]([OH:15])=[O:14]>>[CH3:10][CH:11]([CH:12]([C:1]([OH:3])([CH3:2])[C:4]1[CH:5]=[N:6][CH:7]=[CH:8][CH:9]=1)[C:13]([OH:15])=[O:14])[CH2:16][CH3:17]

Participants

Reactant 2

HCID 77553-Methylpentanoic acid

HCID 95893-Acetylpyridine

Product 1

HCID 19876561HCID 19876561, compound

Procedure

Analysis of the pyrolyzate by preparative thin layer chromatography indicates that the product mixture contains 810 milligrams (54%) of a 1:1 mixture of 3-acetylpyridine and 3-methylvaleric acid.

Sources & evidence

ORD record: ord-f73b3fc809f344b4a9a745dcae8a3e70
Source dataset: uspto-grants-1992_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05148817

Reaction notes

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