HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-[3-Chloro-2-(methylsulfonylaminocarbonyl)phenoxy]-4,6-dimethoxy-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methanesulfonamide | HCID 72879 | — |
| Reactant | 4-Nitrophenyl 2-chloro-6-(4,6-dimethoxy-1,3,5-triazin-2-yloxy)benzoate | HCID 19876598 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2-[3-Chloro-2-(methylsulfonylaminocarbonyl)phenoxy]-4,6-dimethoxy-1,3,5-triazine | HCID 19876585 | — |
Reaction Steps
This compound is prepared in a manner analogous to that of Example 1, Step I, using equimolar amounts of 4-nitrophenyl 2-chloro-6-(4,6-dimethoxy-1,3,5-triazin-2-yloxy)benzoate, methanesulfonamide, and potassium carbonate in acetonitrile to yield 2-[3-chloro-2-(methylsulfonylaminocarbonyl)phenoxy]-4,6-dimethoxy-1,3,5-triazine, Compound 38 of Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05149357 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-dd503b8761c34973817f58b1c0ee42ef |
| Source note | uspto-grants-1992_09 |