Diisobutylamine → Lithium diisobutylamide

HRID 1885990Notes

Reaction equation

HRID 1885990 reaction equation
[CH2:1]([NH:5][CH2:6][CH:7]([CH3:9])[CH3:8])[CH:2]([CH3:4])[CH3:3].C([Li:14])CCC>C1(C)C=CC=CC=1>[CH2:1]([N-:5][CH2:6][CH:7]([CH3:9])[CH3:8])[CH:2]([CH3:4])[CH3:3].[Li+:14]

Participants

4

Reactant 2

HCID 8085DiisobutylamineHCID 178418339Butyllithium

Product 1

HCID 11018925Lithium diisobutylamide

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

4 ml. of diisobutyl amine was added to a 2.0M solution of n-butyl lithium in toluene. A clear solution was obtained of lithium diisobutylamide.

Sources & evidence

ORD record
ord-69140ae5825e41de935615b1f49f0d16
Source dataset
uspto-grants-1992_09
Patent number
US05149457

Reaction notes

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