HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178481704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Trifluoroacetyl fluoride | HCID 67716 | — |
| Reactant | N-Methylhydrazinecarbothioamide | HCID 2723853 | — |
| Product | HCID 178481704 | HCID 178481704 | — |
Reaction Steps
This exemplified compound may be readily synthesized by the reaction of methyl isocyanate with hydrazine to give 4-methyl-3-thiosemicarbazide followed by cyclocondensation with trifluoroacetic acid as described in U.S. Pat. No. 4,477,459. This compound may also be prepared by the reaction of 4-methyl-3-thiosemicarbazide with trifluoroacetylfluoride and heat (U.S. Pat. No. 3,780,052).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05149620 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-b98c545d21194b3c89942f661b4ae0d1 |
| Source note | uspto-grants-1992_09 |