HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53917442, compound → HCID 19876839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53917442 | HCID 53917442 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Product | HCID 19876839 | HCID 19876839 | 99.3% |
Reaction Steps
A mixture of the product of Step 1 (25 g, 85 mmol) and 10% Pd/C (2.5 g) in THF/EtOH (100 ml each) was hydrogenated at 40 psi for 5 hrs. The mixture was filtered through celite and concentrated to give 25 g of the title compound, which was used as such for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05149703 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-60ad59314c1345acb359d589cf90b689 |
| Source note | uspto-grants-1992_09 |