Dichloromethane → HCID 57212210, compound

HRID 1886110Notes

Reaction equation

HRID 1886110 reaction equation
[O:1]1[C@H:5]([C:6]2[CH:11]=[CH:10][CH:9]=[C:8]([CH3:12])[CH:7]=2)[C@H:2]1[CH2:3][OH:4].C(Cl)Cl>CCCCCC.C(OCC)(=O)C>[O:1]1[C@H:5]([C:6]2[CH:11]=[CH:10][CH:9]=[C:8]([CH3:12])[CH:7]=2)[C@H:2]1[CH:3]=[O:4]

Participants

4

Reactant 2

HCID 6344DichloromethaneHCID 54327905HCID 54327905, compound

Product 1

HCID 57212210HCID 57212210, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

The title compound is prepared analogously to Example 5a) from (2R,3R)-2,3-epoxy-3-(3-methylphenyl)-propanol; light-yellow oil. IR (methylene chloride): 2920, 2820, 1730, 1610, 1140, 1070 cm-1 ; Rf =0.49 (hexane/ethyl acetate 3:2).

Sources & evidence

ORD record
ord-5f7e5bb68a1240c18ec38d7c89c55eb2
Source dataset
uspto-grants-1992_09
Patent number
US05149717

Reaction notes

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