HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → HCID 19877066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Tetrafluoroboric acid | HCID 28118 | — |
| Reactant | Bis(p-chlorobenzyl) sulphide | HCID 90172 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19877066 | HCID 19877066 | 80% |
Reaction Steps
5.66 g (20 mmol) of di-(4-chlorobenzyl) sulfide are reacted with 2.6 g (24 mmol) of benzyl alcohol and 8.13 g (50 mmol) of 54% by weight HBF4 in 20 ml of methylene chloride as described in Example 3a). 7.44 g (80% of theory) of di-(4-chlorobenzyl)-benzylsulfonium tetrafluoroborate are obtained as white crystals of melting point 123°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05149767 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-a0714f04b6cb43b0ada5ba63a70b4677 |
| Source note | uspto-grants-1992_09 |