HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glyoxal → HCID 15099950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glyoxal | HCID 7860 | — |
| Reactant | Propylphosphane | HCID 14647240 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15099950 | HCID 15099950 | — |
Reaction Steps
Following the procedure of Example 1, mono-n-propylphosphine, in tetrahydrofuran, as solvent, is reacted with a 40% aqueous glyoxal solution, to give 1,4-di-n-propyl-2,3,5,6-tetrahydroxy-1,4-diphosphorinane, a solid melting at 131°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05149878 |
| Source dataset | uspto-grants-1992_09 |
| ORD ID | ord-4a9086e58ffb49da91792f639302de2c |
| Source note | uspto-grants-1992_09 |